Aside from sulfur, NO is one of the most undesirable substances in exhaust gas after-treatment. It is formed by the splitting of NO2 in the cylinder and a chemical reaction with O2 at high cylinder temperatures. Suppression of NOx formation, like reduction in exhaust after-treatment, is the main task of engine and catalyst developers. Whatever the strategy, be it, for example, low-temperature combustion, exhaust gas recirculation (EGR), post-injection to form enough HC for catalytic reduction, or SCR technology with decomposition of urea into ammonium molecules, to achieve optimization under volatile conditions these highly dynamic and heavily temperature-dependent reactions require the rapid measurement of a wide range of components.